Abstract: Non-crystalline zinc coatings were prepared by mechanically deposition method. XRD was employed to analyze the phase of the coating. The results show that the mechanically deposited non-crystalline zinc coating is a zinc matrix multiple phase metallic mixture of zinc,tin,iron;has no any alloy of compounds,solid solution or metal oxide formed in building of the coating. Zinc powders have no indications of grain refinement in building of the coating.